Contents Preface Introduction Section 1 Purpose, requirements and rules of physical chemistry experiments Section 2 Safety protection of physical chemistry experiments Section 3 Errors and data processing in physical chemistry experiments Section 4 Computer processing of physical chemistry experiment data Combined experiment Ⅰ Experiment 1 Determination of the heat of combustion of sucrose by constant volume thermal method Experiment 2 Determination of the molar mass of sucrose by freezing point depression method Experiment 3 Determination of the rate constant of the acid-catalyzed conversion reaction of sucrose by optical rotation method Experiment 4 Determination of the Michaelis constant of sucrase by spectrophotometry Combined experiment Ⅱ Experiment 5 Determination of saturated vapor pressure of ethyl acetate by static method Experiment 6 Evaporation and condensation method to draw the equilibrium phase diagram of ethyl acetate-ethanol two-liquid system Experiment 7 Determination of the rate constant and activation energy of ethyl saponification by conductivity method Experiment 8 Determination of the dipole moment of ethyl acetate by the solution method Combined experiment Ⅲ Experiment 9 Determination of standard entropy and sublimation enthalpy of crystal iodine Experiment 10 Determination of I2 distribution coefficient anddissociation constant Experiment 11 Determination of the order of acetone iodization reactions Experiment 12 “Iodine Clock” reaction Combined experiment Ⅳ Experiment 13 Determination of partial molar volume of NaCl Experiment 14 Determination of osmotic pressure of NaCl injection Experiment 15 Phase analysis of X-ray powder diffraction method of NaCl Experiment 16 Drawing of three-component equilibrium phase diagram of KCl-HCl-H2O Experiment 17 Determination of the heat of solution for KNO Combined experiment Ⅴ Experiment 18 Production and application of thermocouple Experiment 19 Drawing of two-component metal phase diagram Experiment 20 Determination of the electromotive potential of the original battery Experiment 21 Surface modification and coloration of aluminum anodization Experiment 22 Pyrophosphate copper plating Experiment 23 Stainless steel electrolytic polishing and waste liquid treatment Experiment 24 Synthesis, characterization and electrical properties of silver nano cables Combined experiment Ⅵ Experiment 25 Determination of surface tension of solution Experiment 26 Determination of critical micelle concentration of surfactants Experiment 27 Preparation and stability of sol Experiment 28 Determination of sol electric potential Experiment 29 Preparation and properties of emulsion Experiment 30 Determination of the average molar mass of polymer compounds Combined experiment Ⅶ Experiment 31 Determination of magnetic susceptibility Experiment 32 Biomineral and biomineralization Experiment 33 Synthesis and structure analysis of KDP crystals Experiment 34 Molecular model and crystal structure References Appendix 1 Special topic of physical chemistry experiment technology Special Topic Ⅰ Temperature measurement technology and instruments Special Topic Ⅱ Pressure measurement technology and instruments Special Topic Ⅲ Density measurement technology and instruments Special Topic Ⅳ Electrical measurement technology and instruments Special Topic Ⅴ Optical measurement technology and instruments Special Topic Ⅵ Viscosity measurement technology and instruments Appendix 2 Data sheets commonly used in physical chemistry experiments
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